Chemistry Form One Notes – The Scientific Procedure
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‘The Concept of Scientific Procedure
Explain the concept of selene procedure
The scientific method (procedure) is a process that scientists use to ask questions and conduct
investigations to find answers to these problems. It is logical approach to prablem solving by observing
and collecting data, formulating hypotheses, testing hypotheses, and formulating theories that are
supported by data. The scientific method provides a standardized way for scientists to conduct thet work
However, many scientists work according o other methods as well,
‘THE IMPORTANCE OF THE SCIENTIFIC PROCEDURE
Explain the importance ofthe scenic procedure
Includes
1. The scientific procedure makes a researcher or an experimenter more systematic and organized
‘when investigating r solving a problem,
2. It gives a means by which one can get a solution to several questions about natural phenomnen,
why does water expand when it feezes?
3, Ttmay lead to discoveries and innovations
4 Provides background knowledge upon which Future references may be made
‘5. Itmakes our sense organs more effective in exploring ou natural world, That is, we Become more
sensitive to environmental changes
6. Itmakes us use the available resources mor sustainable in solving everyday problems.
7. Assists us in predicting the future outcome based on the present condition.
‘8 Assists us in testing the validity othe possibility of an event, phenomenon or problem,
“The main steps ofthe scientific procedure
Each Step ofthe Sciemific Procedure
6
Describe each sep ofthe scienfc procedure
Observation (identification) oF statement ofthe problem
‘The frst step ofthe scientific procedure isto identify a researchable problem. A problem isan obstacle
that makes it difficult to achieve a desired goal, objective or purpose. It refers toa situation, condition or
{issue that is unresolved. Observation refers to identification ofa chemical phenomenon, This may include
observing the colour, smell texture of a substance, and so on. Observing involves the use of Senses to
obtain information. Observation is more than the bare fat of observing. It is determined by use of five
senses namely, smell, touch, taste, vision and hearing. For example, o identify the colour of a substance
you have tose it with your eyes. The same case applies to detection of the smell ofa substance or gas
produced by reacting substances in laboratory. To beable to detect the smell of a gas you have to se
{your nose to smell it
(Observation helps a scientist to identify problem. Observation may involve making measurements and
collecting data The data may be descriptive (qualitative) or numerical (quantitative) in nature. Numerical
information such as the fact tha sample of sulphur powder measures 50g is quantitative. Non-mumerical
‘information, such asthe fact thatthe colour of anhydrous copper (ll) sulphate is white, i qualitative.
(Once you identify a problem, it becomes easy to state it scientifically, For example, you can observe that
‘when you puta given volume of water in a narrow container and expose it to open air, it takes much
Jonge to evaporate and decreas in volume, However, when you pu the same amount of water in a wide
container, it takes a much shorter time todo so. This phenomenon can be investigated scientifically
Hypothesis formulation
‘Afler identifying and stating the problem, you can formulate a testable hypothesis for that problem. A
hypothesis isa statement Ii a prediction or proposed solution toa problem based on prior knowledge or
own information about @ chemical phenomenon. It is a logical guess about the outcome of the
experiment. A hypothesis must be able to be tested, Therefore, a hypothesis ean be described a
tentative explanation for an observation, phenomenon, or scientific problem that can be tested by further
lnvestigation. It can be rejected, modified, or accepted only after conducting an experiment to prove or
Aisprove it
Let us take an example of water atthe previous stage. It was observed that the water held in a wide
container evaporated faster than that ina nartow container. Based on what we know about evaporation
(prior knowledge) we can formulate a hypothesis pertaining to this phenomenon. Iis wll known that one
a
ofthe factors affecting the rate of evaporation isthe surface area, From this fact, we can formulate a
testable hypothesis which sates that “evaporation of water nereases with increase in surface area ofthe
comainer in which thar water is placed. This is just a statement. I can be proved wrong or correct by
Setting up and doing an experiment, Remember that this is just an example, though not very much related
to chemistry, We can turn to another relevant example as well
Now, let us look at an example of anhydrous copper (It) sulphate. The anhydrous salt isin powder form.
‘When you expose this salto open ai, it changes is colour and shape, fom is original white powder to
blue crystals, Why does this happen? From our knowledge of the properties ofthis salt (prior knowledge
‘or information gathered) when is placed in open a, it absorbs water vapour from the ar. Iis this water
‘vapour which it absorbs that tums it blue. We ean go as far as formulating a hypothesis, which states
that “When white anhydrous copper (I) sulphate power is exposed to open air, absorbs water vapour
rom the air and turns ino blue crystal”. We sll have a doubt about this hypothesis. How do we know
thatthe liquid absorbed by the sal is telly water? To accept or reject this hypothesis, we must conduct an
experiment
Experimentation
‘Afler making a hypothesis, the next step isto plan and conduct an experiment, Planning an experiment
involves writing down steps for an experiment that will answer the question. It should be remembered
that experimental plan should include short and clear steps It should also include the materials and
‘methods that will be used inthe experiment. These may include safety gers such as gogles, gumboos,
loves, ee, It must also state all expected hazards to be accompanied with the reacting substances or
chemical phenomena being experimented. This could either occu as a result of mishandling chemicals or
apparatus, improper experimental procedure or even testing the pret obained from the experiment
In the scientific method, an experiment is a set of observations (qualitative or quantitative) made in the
context of solving a particular problem or question. An experiment is conducted in order to retain of
falsify a hypothesis conceming a particular phenomenon, The experiment is a basis in the practical
approach to acquiring deeper knowledge about the chemical wold
Experimenting involves carrying out a procedure under controlled conditions in order to. make
observations and collet data To lear moe about mater, chemists stay systems. A system isa specific
Portion of matter in a given repion or space that has been selected for study during an experiment or
‘observation. When you observe a feation in a est tbe, the tes tube and is contents form a system.
4“
‘Your experiment es whether your hypothesis fie. ts important fr your experiment tobe &
fur test. You conduct fr test by mkng se hat you change only one factor ata ime while Keping
alee condions the same (constant). Tes ators at lo called variables. They arth factors that
affect the problem you want to investigate. They can change or be changed during the experiment. Sch
factors inl temperatue, volume, see, ight, cocenatin ight
¢ Ld
é Wy
4
ay *.
Snadntscondcting an experiment
There artes types of varibles These ae
+ Dependent variable: This sth fcr tat changes it value when the values ofthe ther
variables change. is the vale being measured
Independent variable: This isthe fitor tats manutd so so obtain diferent values
+ Controle (or constant) variable: Tis isthe fcr that docs ot change, oi kept constant alt
the time Ht oes not ae the res of the experiment
For example, you might be interested to camy out an experiment to determine the inlence ofthe
conection of phosphors fiir on maize growth To gst the rt esl, you grow maize in sila
conditions of sil and atmosphere envionment (conoid arable) but vary the quantity of eer in
cach et independent variable. Then you meas the eight of maize plans dependent alae afer
2 eri teal ftime a shown in igure blow. The vale ofthe eight you wil obtain wil obviously
depen on he amount concentration) ofthe eile appli This i typical txt. However, most
chemistry experiments do ot involve fret
ra
[Now, lt us tum back to. our experiment Inthe example of determining whether the surfce area increases
the ate of evaporation or not, we ean design an experiment to prove or disprove tis phenomenon. This is
conducted by filing a basin (with large surface area) and a bucket (with small surface area) with 10 lites
of water cach. Then the two containers are placed in open air for 3 days. Here, care must be taken to place
both containers under similar environmental conditions. Containers must be of the same type, that is, both
rit be plastics, metals, ee. In addition, the water used must be obtained from the same source
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cre 50 phorphonsfriizer
1s 28% phosphons enlier
10% phosphors ferlzer
s 10
fetta
. sw mw 3
Time
The effec of frlizeron plant growth
“The only variable tobe kept constant isthe volume of water, which is sett the volume of 10 lites. You
should repeat your experiment several times to make sute thatthe first results were not jus an accident.
Determination ofthe effect of surface area on the rat of evaporation of water
so
Observation and collection of data
Observation and recording of data must be done from the beginning to the end of the experiment Data is
the information gathered during the experiment. This can include descriptive (qualitative) and numerical
(quantitative) data. Numerical data is that which can be measured, for example, 10 lies of water, Sg of|
copper, a five centimetre long ribbon of magnesium, ec. Qualitative data include information that cannot
bbe measured, eg colour, shape or appearance, smell, fel, etc. Recording data is an important part ofthe
Scientific method because it helps sciemists organize thet ideas and observations. Chants, graphs, lists
diagrams, tables and even sketches ate all the ways of recording data during experiments, Records
appearing in the form of tables are easy to read, understand and interpret
Continuing with our hypothetical experiment for determining the effect of surface area onthe rate of|
evaporation, we expet that at the end ofthe experiment the volume of water in each container will have
Aropped to a certain extent
We also expect that the volume of water lost fom the basin willbe bigger than that los rom the bucket.
‘This means that more water will evaporate ftom the basin than from the bucket. Considering that
scenario, we can then predict what the data can be lke. Let ws take this model asa real experiment and
assume the kindof results that could be observed and collected during the experiment.
‘Afler 3 days of the experiment, water from each container was measured. The results obtained were
summarized in the following table
Source: hypothetical
ata collected from evaporation experiment afer 3 days
Amount of water Type ofcomainer
Basin Bucket
Initial volume Final volume 10 tres 70 lies 10 liees 85 lies
Amount of water lost,
(evaporated off) 30lites 1S lies
st
ata analysis and interpretation
(Once your experiment is complete and after you have collected data, you analyse your data tose if your
hypothesis is truco fs. In table 41, we find that, atthe end ofthe experiment, 3 lites of water had
evaporated off from the basin as compared to 1 ites from the Bucket. What does this data tll us? What
{sitrying to reveal? This means that from the basin with large surface area) water evaporated faster than
that from the bucket (with small surface area). The data reveals the fact that surface area plays @ major
role in evaporation of water and many other liquid substances
However, you may sometimes get unexpected results. You may find tht your hypothesis was false. In
such a cas, you will construct a new hypothesis and start the entire process ofthe scientific method over
‘gain. Even if you find that your hypothesis was true, you may want to test agin ina new way.
Conctuson
“The lst tage (at this level of study) ofthe scientific method isto make inferences and draw a conclusion.
Scientists look at the information they gathered and observed. Then they make connections to draw a
comelusion, These conclusions may’be or may not bein agreement with their predictions, Scientists make
incorect predictions all the time. An important part of the scientifie process is to understand why
predictions were incorrect. Many scientists will repeat an experiment Several times to see if they ean
replicate the results before concluding. This ensures that they have conducted the experimen the same
way each time and make sure no introduced errors or ouside Factors affected the experiments outcome,
[Based on data ina hypothetical experiment above, we found that 30 lites of water evaporated fom the
basin (a container with wide mouth and hence a large surface area). At the same time, 1 lites of water
evaporated from a bucket (a container with a narrow mouth and hence a small surface area). From this
result, of course, we can conelude that evaporation of water increases with increase i surface area ofthe
comainer in which thar water is kept. Therefore, our hypothesis is proved true and corect. Remember
always to base your conclusion on the collected and analysed data, though it may deviate, to some extent,
fom the reality for one reason or another.
ADDITIONAL NOTES ON SCIENTIFIC PROCEDURE,
Inadvanced study, the last step ofthe Scientific method is to share what you have learned, Scientists share
information so that others can use the findings to create diferent questions and conduct different
experiments, Sharing information is an important part of working together. Profesional scientists will
s2
publish thei final reports in scientific joumals, magazines, books, or even present their results at
Scientific conferences. For the purpose of study at this evel, the lst stp is conclusion,
[Even though we show the scientific procedure asa series of stps, keep in mind that new information or
thinking might cause a scientist to back up and repeat steps at any point during the process. A process ike
the scientific method tat involves such backing up and repeating is called an iterative process. Therefore,
the siemifi process isan iterative process
Applicaton ofthe scent procedure
“The scientific procedure is used in many areas and in different Fields of study. It is especially applied by
Scientists and researchers to find solutions {0 various scientific problems. Below are some ofthe areas
where the scientific procedure is applied
1 Im scientific researeh: Researchers normally apply the scientific method when conducting,
researches on diverse scientific problems or phenomena. A researchable problem whose solution
is sought for without following the correct sequence ofthe steps ofthe scientific method is not
Tike to get resolved,
2 Ima field study: A field stay (or field work) i offen conducted to find answers to problems or
{est hypotheses. I involves doing some practical work that applies the scientific methods
3. When conducting experiments: An experiment is « methodical procedure carried out withthe
goal of verifying, falsitfing, o establishing the aeuracy of a hypothesis. Experiments vary
greatly in their goals and scale, but always rely on repeatable procedure and logical analysis of
the results
4. Im project work: A project is a planned piece of work that involves careful sty ofa subject or
problem over a period of time, so as to find information onthe subject or problem,
The Scientific Procedure to Carry Out Investigations in Chemistry
Use the Scienifi procedure to cary out investigations in chemistry
In this chaper, we have used two major examples to explain the concept of experimental procedure in
etl. These are the rate of evaporation of water and exposure of anhydrous copper(I) sulphate powder
to open air. Fr casy understanding and quick reference by students the two examples are summarized
33
below. Note thatthe test for the anhydrous copper(I) sulphate powder was not explained in full
However, the summary can give you a good picture on how to go about experimenting it
A. The rate of evaporation of water
Steps
1 Problem/question: Does surface area affect the rate of evaporation of water?
2. Hypothesis: Evaporation of water inreases with increases insure atea
3. Experimentation: A basin and a bucket ate filled with 10 lites of water each. They are left
expose to open air, under similar conditions for a period of 3 days
4. Observation and data collection: Aer 3 days, the remaining water in containers was measured
‘carefully. The results were recorded in table,
5. Date analysis and imterprettion: was found tht 3 lives of water had evaporated frm the
‘asin and 1S lites ffom the bucket From this dat, it was discovered that much water (3 ites)
hhad evaporated from a container with large surface area (basin) as compared to only 1S lites of
‘water that had evaporated ffom a container with a small surface area (bucket).
6 Conclusion: Since a large amount of water evaporated from the basin as compared to that from
the bucket, it is coroct to conclude that surface aca affects the rate of evaporation of water and
‘thatthe larger the surice area the higher i the evaporation, Therefore, the hypothesis i proved
tobe me
‘. Exposure of anhydrous copper (If) sulphate powder to open air
Steps
1. Problem/quesion: Why does anhydrous copper(I) sulphate powder change into hydrated blue
xystals when exposed to open ai?
2. Hypothesis: When exposed to open at, the anhydrous copper (I) sulphate powder absorbs water
‘vapour fom hear and this water vapour turns it to blue erystals
3. Experimentation: The anhydrous sulphate is exposed to open air to absorb sufficient water
‘vapour Then the hydrated sulphates heated to dive out al he Liquid in it
st
4. Observation and data collection: The sample of hydrated blue crystals loses the igidin it and
turns 10 its orginal white powder. The vapour given off s carefully collected, cooled down to
Tiguid, and then putin a beaker or est tbe
5, Data analysis and imerpretaion: The collected liquid is subjected to various water tests to justify
‘whether it is water or just the other liquid substance. The liquid i denied as water
{6 Conclusion: The anhydrous copper (It) sulphate was exposed to air only. We also know tht sit
contains water vapour. Because ofthis reason, iis correct to conclude that the water came from
the water vapour contained in ar. The water ted the white powder to be crystals. Therefore,
‘our hypothesis is tr,
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